Application For Mass Spectrometric Analysis Washington University Resource for Biomedical and Bio-organic Mass Spectrometry Department of Medicine Division of Metabolism and Endocrinology - Box 8127 Washington University School of Medicine 660 S. Euclid Avenue St. Louis, MO 63110 telephone: (314) 362-8190, FAX: (314) 362-8188 PLEASE PROVIDE ALL RELEVANT INFORMATION Investigator:_________________________ Bill to:___________________________ Address:______________________________ ___________________________________ ______________________________________ ___________________________________ ______________________________________ ___________________________________ Telephone:____________________________ Purchase Order No._________________ Type of Analysis (circle one): Low resolution GCMS spectra, 13CO2 breath IRMS, 15N combustion IRMS, 2H218O IRMS, GCIRMS tracer/tracee, GCMS tracer/tracee, GCMS quantitation, Other:____________________________ FOR GCMS SPECTRA Sample formula:_______________________________ Proposed Structure Nominal Mol. Wt.:_____________________________ m.p. or b.p.:_________________________________ Purity:_______________________________________ Wt. sample submitted:_________________________ Soluble in which solvent?_____________________ Is sample stable in solution?_____ Air sensitive?________________________________ Light Sensitive?__________________ Moisture sensitive?___________________________ Heat sensitive?___________________ Refrigerate?__________________________________ Return sample?____________________ FOR IRMS and GCMS TRACER/TRACEE RATIO OR GCMS QUANTITATION: Tracer administrated:_________________________ Tracee to analyze for:____________ Internal Standard Preference:_________________ Sample matrix: plasma, serum, urine, tissue, Other:____________________________________ Sample handling precautions: radioactive, infectious, moiture/heat sensitive. Patient ID Sample date Sample time points Comments, precautions, additional information (Include hazards,handling, helpfull data, questions): __________________________________________________________________________________________________ __________________________________________________________________________________________________ __________________________________________________________________________________________________ IT IS STRONGLY ADVISED TO CONSALT WITH MASS SPECTROMETRY RESOURCE PERSONNEL PRIOR TO SUBMITTING SAMPLES.